Joint Strength with Soldering of Al2O3 Ceramics After Ni-P Chemical Plating

Ni-P alloy was chemically plated on Al2O3 ceramics to produce uniform alloy coatings at temperatures below 70~C. Cu metal was electroplated onto the Ni-P coating to facilitate the soldering and shorten the chemical plating time. Then, the electroplated ceramic specimens were soldered with 60 wt.% Sn-40 wt.% Pb solder in active colophony. The highest shear strength was acquired after the heat treatment at 170℃ for 15 min. The joint fractures mostly propagated along the interface between the ceramics and the Ni-P coating, with some fracture in both the ceramics and the Ni-P coating near the interface and some along the interface between the Cu and Ni-P coatings. The results show that ceramic surface roughness and the chemical plating parameters influence the coating quality, and that suitable heat treatment before the soldering also improves the adhesion between the ceramics and Ni-P coatings, thus strengthening the joints.     

试论综合材质在现代陶艺中的运用

陶瓷艺术已由传统的艺术程式进入了现代艺术表现阶段.在陶瓷艺术中,材质既是一种物质材料,又是重要的艺术表现手段.文章从传统陶瓷材质的单一性到现代陶瓷材质的丰富性为前导,探索综合材质与现代陶艺结合表现的诸多可能性,为现代陶艺表现形式的多样性起到一定的促进作用.     

Application of Reaction-Bonded Silicon Carbide in Manufacturing of Spacecraft Combustion Chamber

Silicon carbide (SiC) ceramics is a good structural ceramics material, which have a lot of excellent properties such as superior high-temperature strength up to a temperature of 1 350 ℃, chemical stability, good resistance to thermal shock and high abrasion resistance. The silicon carbide ceramics material has so far been used widely for manufacturing various components such as heat exchangers, rolls, rockets combustion chamber. Sintering of ceramics structural parts have many technological method, the reac...     

用扩展电阻法研究陶瓷微区电导性能

本文把扩展电阻法应用于陶瓷微区电导性能研究.建立了微区的定位标识系统,可精确、方便地对选定的微区进行电导性能及组分的重复测定.该方法在研究Ba(Sn_(1-x)Sb_x)O_3、ZnO及BaTiO_3半导体瓷应用中得到有意义的结果.     

多孔氧化铝陶瓷内高温流体的流动及传热特性

通过仿真模拟的方法研究了模拟烟气、水蒸气及含尘烟气三类高温流体在多孔氧化铝陶瓷材料内的流动及传热特性。结果表明:随孔隙率增大,流体平均流速加快,流体进出口温降逐渐减小。三类流体中,水蒸气流速最大,在最大孔隙率下其流速达到66.64 m/s;烟气温降最显著,当孔隙率为0.3时,其进出口温差达到最大值85.6 K。随压差的增大,流体流速加快,其中受粉煤灰颗粒影响的含尘烟气流速增幅较小,流速仅从0.23 m/s增至0.93 m/s;另一方面,压差增大导致流体与壁面的热传导减少,模型内流体温降减小。含尘烟气流体扰动较大,当增大孔隙率和压差时,流速呈线性增长;尽管粉煤灰颗粒的存在强化了传热,但流体分子间的相互作用使得含尘烟气温度变化显著。     

混合稀土Nd2O3和CeO2对氧化镁陶瓷硬度及抗热震性能的影响

采用轻质微米级（0.5 μm）MgO粉末为原料,Nd₂O₃、CeO₂为添加剂,聚乙烯醇为黏结剂,以242 MPa压强干压成型,常压1 550 ℃下烧结并保温2 h制得MgO陶瓷,对所得试样进行硬度、抗热震性能、显微结构及物相的测定。先探究不同添加量的单一稀土对MgO陶瓷的硬度及抗热震性能的影响,得到Nd₂O₃和CeO₂的最佳添加量ω分别为3%、8%。然后探究混合稀土Nd₂O₃和CeO₂对MgO陶瓷的性能影响,结果表明混合稀土添加总量ω为3%,Nd₂O₃与CeO₂的质量比为3∶7时,氧化镁陶瓷具有最好性能,硬度值为68 HRA,抗热震次数高达19次。     

基于掺铕钨酸盐荧光强度比的非接触温度传感

为了突破传统测温技术应用的局限性,利用NaY （WO₄）₂：Eu³⁺玻璃陶瓷（glass ceramics,GC）实现了具有非接触、实时响应、自校准等优势的双模荧光强度比（luminescence intensity ratio,LIR）测温。采用高温熔融淬灭法制备出含NaY （WO₄）₂：Eu³⁺纳米晶的透明GC样品,并进行系列光谱测量和热敏性能分析。结果表明,样品中Eu³⁺的激发态能级⁵D₁和⁵D₀和基态能级⁷F₂和⁷F₀为两对独立的热耦合能级,可分别基于这两对热耦合能级实现性能优异的双模LIR温度传感。该双模LIR测温技术数据可靠、测温范围广、灵敏度高,再结合GC材料优势,是可用于光纤温度传感器的核心技术材料。     

一种压电复合材料层合板机电耦合有限单元

基于压电复合材料层合板经典理论,建立了一种四边形机电耦合有限单元．所建单元具有ｍ个电自由度,可直接模拟单元中的电压作用和检测电压输出;单元每一节点具有５个位移自由度,可计及复合材料层合板的拉弯耦合变形．给出了各类刚度矩阵的形式,简述了利用Ｈａｍｉｌｔｏｎ原理推导出机电耦合基本运动方程的过程,并根据所推导的有限元素和基本方程编制了程序并进行了计算,所得结果与文献中的计算和试验结果相吻合．     

压电材料平面问题应力强度因子的边界元计算

从压电介质的基本方程出发,利用功的互等原理,推导了边界积分方程．利用边界元分区算法研究了压电材料无限大平面含中心裂纹的断裂计算,在裂纹尖端采用１／４面力奇异单元,分别计算了应力强度因子ＫⅠ、ＫⅡ和电强度因子Ｋｅ,并讨论了电强度因子Ｋｅ随电载荷的变化规律．计算结果和理论解相吻合．     

新型压电陶瓷涡街流量计

介绍一种新型的压电陶瓷涡街流量计,该流量计采用ＢＳＴ压电陶瓷元件来检测旋涡释放频率,使该流量计能在高温工况下工作,一年多的工业现场运行试验结果表明,新研制的涡街流量计可靠性高、稳定性好,在４００℃高温和１０ＭＰａ高压下能长期连续正常运行。